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  • Ramped Pyroxidation Radiocarbon Dating of Lime Mortar

Ramped Pyroxidation Radiocarbon Dating of Lime Mortar

PROJECT OVERVIEW

A ramped pyroxidation laboratory has been established at 14CHRONO to develop novel applications in the field of radiocarbon dating. One such application is the ability to extract and date CO2 from lime-based mortars, providing a new technique for understanding the chronology of our built heritage.

This project, still on-going, has the following aims:

  • Validate that the approach on materials of known age
  • Examine the working limits of the method on a range of mortar types
  • Application of the method to archaeological materials of interest and demonstration of the value of this application to our understanding of built monuments

This research has been carried out in collaboration with colleagues at the Centre for Community Archaeology (QUB) and from a number of international universities and institutions, including Åbo Akademi University, Finland, and Aarhus University, Denmark. The laboratory is one of a handful of labs leading the development of mortar dating and collaborating in an international mortar dating intercomparison study (MODIS 2) led by colleagues at ETH Zurich.

The project is also actively engaged in outreach, working with local community groups (Derry Tower Heritage Group), archaeological societies (Dover Archaeological Group, Canterbury Archaeological Trust) and government bodies (Historic Environment Division, Department for Communities).

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Impact of Research

The project has had both academic impact and non-academic impact. Academic impact has been achieved through demonstration of the successful dating of mortars of known age with the technique. This has opened up further avenues of research and collaborations with archaeologists and has generated considerable interest in those wishing to submit mortar samples for analysis. The research and results have also resulted in a number of articles in leading archaeological journals (Journal of Archaeological Science, Archaeometry), in turn leading to continued funding for on-going projects (Royal Irish Academy Archaeology Research Grant).


Societal impact has been achieved, for example, in the work carried out in collaboration with the Derry Tower Heritage Group. This resulted in the discovering of a previously unknown Irish round tower, the last known remaining monastic medieval building in the city of Derry. This finding received considerable news and press coverage, for example, featuring on RTE News (Ireland’s state broadcaster) and the BBC News website. Plans are in place by Derry Tower Heritage Group to develop the site and monument for the benefit of locals, visitors and tourists. Work is also on-going on a project to date the round towers of Northern Ireland, in collaboration with the Historic Environment Division, Northern Ireland, and the Royal Irish Academy, Republic of Ireland. The results of this work will have significant impact when completed.

Major grants and funding

Royal Irish Academy 2020 Archaeological Research Grant for “Northern Ireland’s Round Towers (NIRT): Establishing a Chronology and Technological Understanding through Mortar”

Publications

Recent papers:

Barrett, G. and Donnelly, C. 2019. Hiding in plain sight. Archaeology Ireland. 33 14-17.

Barrett, G. T., Donnelly, C., and Reimer, P. J. 2020. Radiocarbon dating mortar: the identification of a medieval Irish round tower using a multi-method inter-comparative approach. Journal of Archaeological Science: Reports. 33 102538

Barrett, G. T., Keaveney, E., Lindroos, A., Donnelly, C., Daugbjerg, T. S., Ringbom, A., Olsen, J. and Reimer, P.J. 2011. Ramped pyroxidation: a new approach for radiocarbon dating of lime mortars. Journal of Archaeological Science. [Accepted]

Daugbjerg, T. S., Lindroos, A., Heinemeier, J., Ringbom, Å., Barrett, G., Michalska, D., Hajdas, I., Raja, R. and Olsen, J. 2021a. A field guide to mortar sampling for radiocarbon dating. Archaeometry. [Early View] doi.org/10.1111/arcm.12648

Collaborators

The project includes a collaborative research team as follows: 

Alf Lindroos
Faculty of Science and Technology, Åbo Akademi University, Turku, Finland

Colm Donnelly
Centre for Community Archaeology, School of Natural and Built Environment, Queen’s University Belfast, Elmwood Avenue, Belfast BT7 1NN, Northern Ireland, UK

Thomas Schrøder Daugbjerg
Aarhus AMS Centre (AARAMS), Department of Physics and Astronomy, Aarhus University, Aarhus, Denmark

Åsa Ringbom
Art History, Åbo Akademi University, Turku, Finland

Jesper Olsen
Aarhus AMS Centre (AARAMS), Department of Physics and Astronomy, Aarhus University, Aarhus, Denmark

Danuta Michalska,
Institute of Geology, Adam Mickiewicz University Poznan, Poland

Irka Hajdas,
Laboratory of Ion Beam Physics, ETH Zurich, Switzerland

Stephen Donnelly
Derry Tower Heritage Group, Derry, Northern Ireland

 

Find out more
  • Dr. Gerard Barrett
    14CHRONO,
    School of Natural and Built Environment,
    Queen’s University Belfast
    g.barrett@qub.ac.uk 

RELATED NEWS ARTICLES

  • RTE News Excerpt:
    https://www.rte.ie/news/player/2018/0928/21439384-derry-landmark-thought-to-have-been-17th-century-windmill-is-medieval-round-tower/ 

  • BBC News Article:
    https://www.bbc.co.uk/news/uk-northern-ireland-foyle-west-45692121

  • Current Archaeology Magazine article:
    https://archaeology.co.uk/articles/news/hiding-in-plain-sight-a-lost-medieval-tower-in-derry.htm 

 
 
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