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PhD Opportunities

Liquid Coordination Complexes for the Synthesis of Semiconductor Nanoparticles

School of Chemistry and Chemical Engineering | PHD

Applications are now CLOSED
Funding
Funded
Reference Number
SCCE-2022-001
Application Deadline
25 February 2022
Start Date
3 October 2022

Overview

Liquid coordination complexes (LCCs), also known as ionic liquid analogues, are a new class of liquid materials with very high metal contents, typically prepared from metal salts and simple organic donors (ligands). LCCs combine all the advantages of ionic liquids (liquidus range of >200 °C, good conductivity and impressive solvating properties) with much lower price, high metal content and versatility in terms of metal coordination. In this project, new LCCs will be developed and investigated as precursors for the ionothermal synthesis of III/V semiconductor nanoparticles, applicable for solar energy conversion.

The student will acquire a very broad set of skills in inorganic and materials chemistry: working with air-sensitive materials (Schlenk line and glovebox), ionothermal synthesis (microwave reactor and microfluidic reactor), as well as characterisation of liquid coordination complexes (Raman and multinuclear NMR spectroscopy). In collaboration with the school of Maths and Physics, the student will have access to a unique in operando TEM liquid cell, where the nanoparticle formation can be studied in situ. These in-house techniques will be complemented by EXAFS studies at Diamond Light Source. This project will be co-supervised with Professor John Holbrey.

Candidates must possess or expect to obtain, a 2:1 or first-class degree in Chemistry, Engineering or Physical Sciences related discipline

Funding Information

The studentships detailed are open to UK and ROI nationals, or EU nationals that have obtained settled status in the UK. Full eligibility information can be viewed via: https://www.nidirect.gov.uk/articles/department-economy-postgraduate-studentship-scheme

Project Summary
Supervisor


    Mode of Study

    Full-time: 3 years


    Funding Body
    Department for Economy
    Apply now Register your interest

    Chemistry overview

    The School of Chemistry and Chemical Engineering aims to promote sustainable processes and materials to meet the energy and healthcare demands of the future. The School is expanding rapidly and this is creating many new and exciting research opportunities with over £15m being invested to develop and expand the core research areas of catalysis, biological and medicinal chemistry, and materials.

    Mode of study / duration

    Registration is on a full-time or part-time basis, under the direction of a supervisory team appointed by the University. You will be expected to submit your thesis at the end of three years of full-time registration for PhD, or two years for MPhil (or part-time equivalent).

    Key Facts

    QUB is a member of the Russell Group of the UK’s 24 leading research-intensive universities.

    • QUB is joint 1st in the UK for Research Intensity for Chemistry (Complete University Guide 2021)
    • QUB has been placed joint 8th in the UK for research intensity (REF 2014/ Times Higher Education)
    • QUB is ranked in the top 25 universities in the world for international joint publications (U-Multirank 2020)
    • QUB is ranked 43 in the world in the Times Higher Education Impact Rankings 2021

    Course content

    Research Information

    Associated Research
    Much of our research falls under the broad headings of Healthcare and Sustainability, examples of recent funded projects include development of novel antibiotics and reduction of single use plastics. The School also leads the EU-funded Bryden Centre for renewable energy research, the industry-led Centre for Advanced Sustainable Energy (CASE) as well as our world-leading QUILL ionic liquids research centre. Students trained in our School are equipped with the skills that allow them to go out and make a real difference in the world.

    Our areas of interest include adventurous research at the cutting edge of catalysis (where chemistry meets other disciplines, especially engineering, innovative Molecular Materials and Functional Materials), ionic liquid technology (‘super solvents' which do not form vapours and can be used as non-polluting alternatives to conventional solvents) and Synthesis and Biological Organic Chemistry (working to deliver compounds addressing the regulation of cellular functions).
    QUILL (Queen's University Ionic Liquid Laboratories): the largest multidisciplinary research group in the world centred on ionic liquid technology, whose work on ‘super solvents' (which do not form vapours and can be used as non-polluting alternatives to conventional solvents) was voted ‘Most Important British Innovation of the 21st Century' in 2013.
    All of our research groups have significant links with researchers and other institutions globally, and there are opportunities for collaboration and study visits, etc.
    We have extensive links with industry, meaning that employment prospects for our graduates are excellent.
    Much of our research is interdisciplinary, and our students can broaden their experience and knowledge by working with researchers from other disciplines (eg biologists, physicists).

    Career Prospects

    Introduction
    For further information on career opportunities at PhD level please contact the Faculty of Engineering and Physical Sciences Student Recruitment Team on askEPS@qub.ac.uk. Our advisors - in consultation with the School - will be happy to provide further information on your research area, possible career prospects and your research application.

    People teaching you

    Dr Mark Muldoon
    Director of Postgraduates
    Chemistry&Chemical Engineering
    Email: m.j.muldoon@qub.ac.uk

    Learning Outcomes

    Course structure

    -

    Entrance requirements

    Graduate
    The minimum academic requirement for admission to a research degree programme is normally an Upper Second Class Honours degree from a UK or ROI HE provider, or an equivalent qualification acceptable to the University. Further information can be obtained by contacting the School.

    International Students

    For information on international qualification equivalents, please check the specific information for your country.

    English Language Requirements

    Evidence of an IELTS* score of 6.0, with not less than 5.5 in any component, or an equivalent qualification acceptable to the University is required (*taken within the last 2 years).

    International students wishing to apply to Queen's University Belfast (and for whom English is not their first language), must be able to demonstrate their proficiency in English in order to benefit fully from their course of study or research. Non-EEA nationals must also satisfy UK Visas and Immigration (UKVI) immigration requirements for English language for visa purposes.

    For more information on English Language requirements for EEA and non-EEA nationals see: www.qub.ac.uk/EnglishLanguageReqs.

    If you need to improve your English language skills before you enter this degree programme, INTO Queen's University Belfast offers a range of English language courses. These intensive and flexible courses are designed to improve your English ability for admission to this degree.

    Tuition Fees

    Northern Ireland (NI) 1 £4,596
    Republic of Ireland (ROI) 2 £4,596
    England, Scotland or Wales (GB) 1 £4,596
    EU Other 3 £23,850
    International £23,850

    1 EU citizens in the EU Settlement Scheme, with settled or pre-settled status, are expected to be charged the NI or GB tuition fee based on where they are ordinarily resident, however this is provisional and subject to the publication of the Northern Ireland Assembly Student Fees Regulations. Students who are ROI nationals resident in GB are expected to be charged the GB fee, however this is provisional and subject to the publication of the Northern Ireland Assembly student fees Regulations.

    2 It is expected that EU students who are ROI nationals resident in ROI will be eligible for NI tuition fees. The tuition fee set out above is provisional and subject to the publication of the Northern Ireland Assembly student fees Regulations.

    3 EU Other students (excludes Republic of Ireland nationals living in GB, NI or ROI) are charged tuition fees in line with international fees.

    All tuition fees quoted are for the academic year 2021-22, and relate to a single year of study unless stated otherwise. Tuition fees will be subject to an annual inflationary increase, unless explicitly stated otherwise.

    More information on postgraduate tuition fees.

    Chemistry costs

    Additional course costs

    All Students

    Depending on the programme of study, there may also be other extra costs which are not covered by tuition fees, which students will need to consider when planning their studies . Students can borrow books and access online learning resources from any Queen's library. If students wish to purchase recommended texts, rather than borrow them from the University Library, prices per text can range from £30 to £100. Students should also budget between £30 to £100 per year for photocopying, memory sticks and printing charges. Students may wish to consider purchasing an electronic device; costs will vary depending on the specification of the model chosen. There are also additional charges for graduation ceremonies, and library fines. In undertaking a research project students may incur costs associated with transport and/or materials, and there will also be additional costs for printing and binding the thesis. There may also be individually tailored research project expenses and students should consult directly with the School for further information.

    Bench fees

    Some research programmes incur an additional annual charge on top of the tuition fees, often referred to as a bench fee. Bench fees are charged when a programme (or a specific project) incurs extra costs such as those involved with specialist laboratory or field work. If you are required to pay bench fees they will be detailed on your offer letter. If you have any questions about Bench Fees these should be raised with your School at the application stage. Please note that, if you are being funded you will need to ensure your sponsor is aware of and has agreed to fund these additional costs before accepting your place.

    How do I fund my study?

    1.PhD Opportunities

    Find PhD opportunities and funded studentships by subject area.

    2.Funded Doctoral Training Programmes

    We offer numerous opportunities for funded doctoral study in a world-class research environment. Our centres and partnerships, aim to seek out and nurture outstanding postgraduate research students, and provide targeted training and skills development.

    3.PhD loans

    The Government offers doctoral loans of up to £26,445 for PhDs and equivalent postgraduate research programmes for English- or Welsh-resident UK and EU students.

    4.International Scholarships

    Information on Postgraduate Research scholarships for international students.

    Funding and Scholarships

    The Funding & Scholarship Finder helps prospective and current students find funding to help cover costs towards a whole range of study related expenses.

    How to Apply

    Apply using our online Postgraduate Applications Portal and follow the step-by-step instructions on how to apply.

    Find a supervisor

    If you're interested in a particular project, we suggest you contact the relevant academic before you apply, to introduce yourself and ask questions.

    To find a potential supervisor aligned with your area of interest, or if you are unsure of who to contact, look through the staff profiles linked here.

    You might be asked to provide a short outline of your proposal to help us identify potential supervisors.